Source:Journal of Crystal Growth, Volume 446
Author(s): Kosuke Z. Takahashi, Daisuke Okuyama, Taku J. Sato
Mechanical alloying method has been employed to prepare the Ba-Fe-As-P precursors, necessary for the Ba-(As,P) flux growth of the single crystalline BaFe2(As1−xPx)2. By alloying constituent elementals mechanically, the Ba-(As,P) precursors are successfully formed at the room temperature within one hour, significantly reducing preparation time. Using the mechanically alloyed precursors, we have grown single crystals of BaFe2(As1−xPx)2 with the sizes up to 5mm×5mm×0.1mm.
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